C2120 Analytical Chemistry - laboratory course

Faculty of Science
Spring 2008

The course is not taught in Spring 2008

Extent and Intensity
0/4/0. 4 credit(s). Recommended Type of Completion: graded credit. Other types of completion: z (credit).
Teacher(s)
prof. RNDr. Přemysl Lubal, Ph.D. (seminar tutor)
Guaranteed by
prof. RNDr. Vítězslav Otruba, CSc.
Department of Chemistry – Chemistry Section – Faculty of Science
Prerequisites (in Czech)
Předpokladem je absolvování základních přednášek z Obecné chemie (C1020), Anorganické chemie I (C1061), Anorganické chemie II (C2062), Organické chemie I (C2021), Organické chemie II (C3022) a příslušných laboratorních cvičení z těchto předmětů.
Course Enrolment Limitations
The course is also offered to the students of the fields other than those the course is directly associated with.
fields of study / plans the course is directly associated with
there are 17 fields of study the course is directly associated with, display
Abstract
A systematic training of "classical" analytical chemistry for students of chemistry. The course includes qualitative analysis, gravimetric analysis, and titrimetry.
Key topics
  • QUALITITATIVE ANALYSIS
  • 1. Analytical reactions of Li(I), Na(I), K(I), NH4+, Mg(II), Ca(II), Sr(II), Ba(II).
  • 2. Analytical reactions of Hg2(II), Ag(I), Pb(II), Hg(II), Cu(II), Cd(II), Bi(III), Sb(III), Sn(II), Sn(IV).
  • 3. Analytical reactions of Al(III), Cr(III), Fe(III), Fe(II), Mn(II), Zn(II), Co(II), Ni(II).
  • 4. Analytical reactions of sulphates, sulphites, thiosulphates, fluorides, silicates.
  • 5. Analytical reactions of chromates, phosphates, arsenates, arsenites, borates, carbonates.
  • 6. Analytical reactions of chlorides, bromides, iodides, thiocyanates, hydrogensulfides, nitrites, nitrates, perchlorates. QUANTITATIVE ANALYSIS
  • 7. GRAVIMETRY: Iron determination as Fe2O3.
  • 8. ACID-BASE TITRATIONS: Standardization of standard solutions. a) Standardization of 0,1 M NaOH solution using dihydrate of oxalic acid (fft and mo with CaCl2). b) Standardization of 0,1 M HCl solution using sodium carbonate.
  • 9. ACID-BASE TITRATIONS: Alkalimetry. a) Acetic acid determination. b) Phosphoric acid determination.
  • 10. ACID-BASE TITRATIONS: Acidimetry. a) Ammonia determination. b) Sodium carbonate determination in technical liquor. c) Determination of insoluble carbonate.
  • 11. CHELATOMETRIC TITRATIONS: a) Standardization of 0,05 M EDTA solution using lead nitrate. b) Ni(II) determination. c) Determination of Ca(II) a Mg(II) cations in mixture.
  • 12. REDOX TITRATIONS: Iodometry. a) Standardization of 0,05 M Na2S2O3 solution using KIO3. b) Winkler determination of dissolved oxygen in waters.
  • 13. REDOX TITRATIONS: Bischromatometry. a) Preparation of K2Cr2O7 standard solution. b) Fe(II) determination.
Study resources and literature
  • ŠENKÝŘ, Jaroslav. Kvalitativní analýza : vybrané postupy k důkazu iontů. 2. vyd. Brno: Vydavatelství Masarykovy univerzity, 1995, 76 s. ISBN 8021011726. info
  • ŠENKÝŘ, Jaroslav. Kvantitativní analýza : pracovní návody pro základní cvičení. 1. vyd. Brno: Vydavatelství Masarykovy univerzity, 1995, 44 s. ISBN 8021012145. info
  • Kotuček M., Skopalová J., Příklady z analytické chemie, Vydavatelství UniverzityPalackého Olomouc 1997
Method of verifying learning outcomes and course completion requirements (in Czech)
praktická laboratorní cvičení
Language of instruction
Czech
Follow-Up Courses
Further comments (probably available only in Czech)
The course can also be completed outside the examination period.
The course is taught annually.
The course is taught every week.
General note: Vyučují učitelé katedry analytické chemie.
  • Permalink: https://is.muni.cz/course/sci/spring2008/C2120